Abstract:SHRIMP IIe MC has the characteristics of high resolution, high sensitivity, high precision, trace analysis and in-situ analysis. In-situ istopic analysis within the scope of 20μm can be carried out. Thus, the original property of the determination object can be kept. Zircon oxygen isotopic value of Xishan vein rocks in Linglong gold deposit shows the characteristics of mantle-derived source. It also has the characteristics of crust source. It indicates the contribution of recycled crust or sediments. As showed by SHRIMP UPb zircon dating, rock-forming age of No. 55 vein is (125.80±0.86)Ma, metallogenic age is the early Cretaceous; while rock-forming age of Houdi gold deposit is (142.77±0.96)Ma, and metallogenic age is the early Yanshan.