Abstract:The copper content in copper concentration powder is generally 30%. Iodometric determination of copper concentrate has been listed as national standard methods. Flame atomic absorption spectrometry determination of copper content is generally applied to determing low content copper. Its measuring range is generally 0.001%~5%. In this paper, samples have been decomposited by aqua regia and diluted, in 2% hydrochloric acid medium, using a high concentration standard series atomic absorption rapid determination method, copper content of copper concentration powder has been determined. This method is simple, rapid with good selection and high accuracy.